Providing coverage of design principles for distillation processes, this text contains a presentation of process and equipment design procedures. It also highlights limitations of some design methods, and offers guidance on how to overcome them.

After an overview of the fundamentals, limitations, and scope of reactive distillation, this book uses rigorous models for steady-state design and dynamic analysis of different types of reactive distillation columns and quantitatively compares the economics of reactive distillation columns with conventional multi-unit processes. It goes beyond traditional steady-state design that primarily considers the capital investment and energy costs when analyzing the control structure and the dynamic robustness of disturbances, and discusses how to maximize the economic and environmental benefits of reactive distillation technology.

A timely treatment of distillationcombining steady-state designand dynamic controllability As the world continues to seek new sources of energy, the distillation process remains one of the most important separation methods in the chemical, petroleum, and energy industries. And as new renewable sources of energy and chemical feedstocks become more universally utilized, the issues of distillation design and control will remain vital to a future sustainable lifestyle. Distillation Design and Control Using Aspen Simulation introduces the current status and future implications of this vital technology from the dual perspectives of steady-state design and dynamics. Where traditional design texts have focused mainly on the steady-state economic aspects of distillation design, William Luyben also addresses such issues as dynamic performance in the face of disturbances. Utilizing the commercial simulators Aspen Plus and Aspen Dynamics, the text guides future and practicing chemical engineers first in the development of optimal steady-state designs of distillation systems, and then in the development of effective control structures. Unique features of the text include: * In-depth coverage of the dynamics of column design to help develop effective control structures for distillation columns * Development of rigorous simulations of single distillation columns and sequences of columns * Coverage of design and control of petroleum fractionators Encompassing nearly four decades of research and practical developments in this dynamic field, the text represents an important reference for both students and experienced engineers faced with distillation problems.

The batch distillation process has existed for many centuries. It is perhaps the oldest technology for separating or purifying liquid mixtures and is the most frequently used separation method in batch processes. In the last 25 years, with continuous development of faster computers and sophisticated numerical methods, there have been many published works using detailed mathematical models with rigorous physical property calculations and advanced optimisation techniques to address several important issues, such as selection of column configurations, design, operation, off-cut recycling, use of batch distillation in reactive and extractive modes, etc.Batch Distillation: Design and Operation presents excellent, important contributions of many researchers from around the globe, including those of the author and his co-workers./a

Distillation has historically been the main method for separating mixtures in the chemical process industry. However, despite the flexibility and widespread use of distillation processes, they still remain extremely energy inefficient. Increased optimization and novel distillation concepts can deliver substantial benefits, not just in terms of significantly lower energy use, but also in reducing capital investment and improving eco-efficiency. While likely to remain the separation technology of choice for the next few decades, there is no doubt that distillation technologies need to make radical changes in order to meet the demands of the energy-conscious society. Advanced Distillation Technologies: Design, Control and Applications gives a deep and broad insight into integrated separations using non-conventional arrangements, including both current and upcoming process intensification technologies. It includes: Key concepts in distillation technology Principles of design, control, sizing and economics of distillation Dividing-wall column (DWC) – design, configurations, optimal operation and energy efficient and advanced control DWC applications in ternary separations, azeotropic, extractive and reactive distillation Heat integrated distillation column (HIDiC) – design, equipment and configurations Heat-pump assisted applications (MVR, TVR, AHP, CHRP, TAHP and others) Cyclic distillation technology – concepts, modeling approach, design and control issues Reactive distillation – fundamentals, equipment, applications, feasibility scheme Results of rigorous simulations in Mathworks Matlab & Simulink, Aspen Plus, Dynamics and Custom Modeler Containing abundant examples and industrial case studies, this is a unique resource that tackles the most advanced distillation technologies – all the way from the conceptual design to practical implementation. The author of Advanced Distillation Technologies, Dr. Ir. Anton A. Kiss, has been awarded the Hoogewerff Jongerenprijs 2013. Find out more (website in Dutch)...

Most available books in chemical engineering mainly pertain to continuous processes, with batch distillation relegated to a small section. Filling this void in the chemical engineering literature, Batch Distillation: Simulation, Optimal Design, and Control, Second Edition helps readers gain a solid, hands-on background in batch processing. The seco

A distillation column is both multivariable and nonlinear - and it consumes immense quantities of energy. Yet, despite the desigh challenges it presents, it is still the most popular unit operation for refining in industrial plants today. Much has been published on the subject of distillation column design, but much remains to be explained. That is why this book is unique. In a departure from the more traditional empirical and theoretical approaches, it introduced the reader to the practical realm, by presenting quantitative design techniques that have been demonstrated to be useful and valid over the course of hundreds of actual applications. The book is divided into three main parts. Part I, an introduction, presents an industrial perspective of control objectives. It discusses briefly the relationship between column design features and column controllability. It thus provides a short refresher course for chemical engineers and background for those trained in other branches of engineering. Part II, Concepts and Configurations, discusses column overhead and base arrangements, typical control schemes, and some hardware considerations. Part III is dedicated to quantitative design. Mathematical models are presented for pressure and differential pressure controls, liquid level control, and composition control of binary distillation. Emphasis on topics of primary interest to the control engineer Essentially nonmathematical treatment Ideal for those involved in troubleshooting existing columns as well to design engineers